HH-1毛细管柱工作场所空气中七FU烷、异FU烷、恩FU烷气相色谱测定方法
HH-1毛细管柱工作场所空气中七FU烷、异FU烷、恩FU烷气相色谱测定方法 详细信息：
名称：毛细管柱
固定相：二甲基聚硅氧烷
规格：30m*0.32mm*1.0um
型号：HH-1
浩瀚色谱（山东）应用技术开发有限公司建立工作场所空气中七氟wan、异fu烷、恩氟wan溶剂解吸气相色谱测定的方法.方法 空气中的七fu烷、异fu烷、恩fu烷采用活性炭管采集,二氯甲烷解吸,经二甲基硅氧烷(hh-1)毛细管色谱柱分离的气相色谱测定方法.结果 本方法七fu烷、异fu烷、恩fu烷质量浓度分别在1.9~304.8 μg/ml、2.1~300.4 μg/ml和1.7~305.2 μg/ml范围内线性关系良好,相关系数均大于0.999,检出限分别为0.6、0.6和0.5μg/ml,定量下限分别为1.9 μg/ml、2.1μg/ml和1.7μg/ml,方法zui低检出质量浓度分别为0.1、0.2、0.1 mg/m(3 按采集空气样品4.5 L计算);七fu烷、异fu烷、恩fu烷的相对标准偏差分别为2.5%~3.0% 、2.3%~3.1% 、2.2%~3.0% ;平均解吸效率分别为 101.1%~103.3% 、100.7%~102.7% 、101.0%~102.9%;七fu烷、异fu烷、恩fu烷穿透容量分别大于3.7、3.4、3.4 mg (100 mg活性炭);采样效率均为;样品在室温下至少可保存10 d.结论 本方法检出限低,准确度高,精密度好,适用于工作场所空气中七fu烷、异fu烷、恩fu烷的测定.
HH-1毛细管柱工作场所空气中七FU烷、异FU烷、恩FU烷气相色谱测定方法 测试谱图：
HH-1 Capillary Column Determination of HeptaFU, IsoFU and EnFU in Workplace Air by Gas Chromatography
Detailed information of gas chromatographic determination method of heptaFU alkane, isoFU alkane and EnFU alkane in the air of HH-1 capillary column workplace:
Name: capillary column
Stationary phase: dimethylpolysiloxane
Specification: 30m * 0.32mm * 1.0um
Model: HH-1
Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. established a method for the determination of heptafluorowan, isofuane and enflurane in the air of workplaces by solvent desorption gas chromatography Methods The heptafulane, isofulane and enfurane in the air were collected by activated carbon tube, desorbed by dichloromethane, and separated by capillary chromatography with dimethylsiloxane (hh-1) Results The mass concentrations of heptafuane, isofuane and enfurane in this method were 1.9~304.8 μ g/ml、2.1~300.4 μ G/ml and 1.7~305.2 μ The linearity is good within the range of g/ml, the correlation coefficient is greater than 0.999, and the detection limits are 0.6, 0.6 and 0.5 respectively μ G/ml, lower limit of quantification is 1.9 respectively μ g/ml、2.1 μ G/ml and 1.7 μ G/ml, the low detectable mass concentration of method zui is 0.1, 0.2 and 0.1 mg/m respectively (3 calculated according to 4.5 L of collected air sample); The relative standard deviations of heptafuane, isofuane and enfurane are 2.5%~3.0%, 2.3%~3.1% and 2.2%~3.0% respectively; The average desorption efficiency was 101.1%~103.3%, 100.7%~102.7% and 101.0%~102.9% respectively; The penetration capacities of heptafuane, isofuane and enfurane are more than 3.7 mg, 3.4 mg and 3.4 mg respectively (100 mg activated carbon); The sampling efficiency is; The sample can be stored at room temperature for at least 10 d. Conclusion This method has low detection limit, high accuracy and good precision, and is suitable for the determination of heptafuane, isofuane and enfurane in the air of workplace
HH-1 Capillary Column Workplace Gas Chromatographic Determination of HeptaFU, IsoFU and EnFU in Air Test Spectrum: