EPA TO-14/TO-15 Rtx-1

1	二氟二氯甲烷	Dichlorodifluoromethane	75-71-8
2	氯甲烷	Chloromethane	74-87-3
3	1''2-二氯四氟乙烷	Dichlorotetrafluoroethane	76-14-2
4	氯乙烯	Vinyl chloride	75-01-4
5	1''3-丁二烯	1''3-Butadiene	106-99-0
6	溴甲烷	Bromomethane	74-83-9
7	氯乙烷	Chloroethane	75-00-3
8	溴乙烯	Bromoethene	593-60-2
9	丙酮	Acetone	67-64-1
10	三氯氟甲烷	Trichlorofluoromethane	75-69-4
11	异丙醇	Isopropyl Alcohol	67-63-0
12	1''1-二氯乙烯	1''1-Dichloroethene	75-35-4
13	二氯甲烷	Methylene Chloride	75-09-2
14	氯丙烯	3-Chloropropene	107-05-1
15	二硫化碳	Carbon disulfide	75-15-0
16	氟利昂® TF	Freon® TF	76-13-1
17	反-1''2-二氯乙烯	trans-1''2-Dichloroethene	156-60-5
18	1''1-二氯乙烷	1''1-Dichloroethane	75-34-3
19	甲基叔丁基醚	Methyl tert-butyl ether	1634-04-4
20	2-丁酮	Methyl ethyl ketone	78-93-3
21	顺-1 ''2 -二氯乙烯	cis-1''2-Dichloroethene	156-59-2
22	溴氯甲烷	Bromochloromethane (IS)	74-97-5
23	正己烷	n-Hexane	110-54-3
24	氯仿	Chloroform	67-66-3
25	四氢呋喃	Tetrahydrofuran	109-99-9
26	1''2-二氯乙烷	1''2-Dichloroethane	107-06-2
27	1''1''1-三氯乙烷	1''1''1-Trichloroethane	71-55-6
28	苯	Benzene	71-43-2
29	四氯化碳	Carbon Tetrachloride	56-23-5
30	环己烷	Cyclohexane	110-82-7
31	1''4-二氟苯	1''4-Difluorobenzene (IS)	540-36-3
32	1''2-二氟苯	1''2-Dichloropropane	78-87-5
33	溴二氯甲烷	Bromodichloromethane	75-27-4
34	三氯乙烯	Trichloroethene	79-01-6
35	1''4-二氧六环	1''4-Dioxane	123-91-1
36	2''2''4-三甲基戊烷	2''2''4-Trimethylpentane	540-84-1
37	正庚烷	n-Heptane	142-82-5
38	顺式-1''3-二氯丙烯	cis-1''3-Dichloropropene	10061-01-5
39	4-甲基-2-戊酮	Methyl Isobutyl Ketone	108-10-1
40	反式-1''3-二氯丙烯	trans-1''3-Dichloropropene	10061-02-6
41	1''1''2-三氯乙烷	1''1''2-Trichloroethane	79-00-5
42	甲苯	Toluene	108-88-3
43	2-已酮	Methyl butyl ketone	591-78-6
44	一氯二溴甲烷	Dibromochloromethane	124-48-1
45	1''2-二溴乙烷	1''2-Dibromoethane	106-93-4
46	四氯乙烯	Tetrachloroethene	127-18-4
47	氯苯-D5	Chlorobenzene-d5 (IS)	3114-55-4
48	氯苯	Chlorobenzene	108-90-7
49	乙基苯	Ethylbenzene	100-41-4
50	50间二甲苯/对二甲苯	m-xylene/p-xylene	108-38-3/106-42-3
51	三溴甲烷	Bromoform	75-25-2
52	苯乙烯	Styrene	100-42-5
53	1''1''2''2-四氯乙烷	1''1''2''2-Tetrachloroethane	79-34-5
54	邻二甲苯	o-Xylene	95-47-6
55	2-氯甲苯	2-Chlorotoluene	95-49-8
56	4-乙基甲苯	4-Ethyltoluene	25550-14-5
57	1''3''5-三甲苯	1''3''5-Trimethylbenzene	108-67-8
58	1''2''4-三甲苯	1''2''4-Trimethylbenzene	95-63-6
59	1''3-二氯苯	1''3-Dichlorobenzene	541-73-1
60	1''4-二氯苯	1''4-Dichlorobenzene	106-46-7
61	1''2-二氯苯	1''2-Dichlorobenzene	95-50-1
62	1''2''4-三氯苯	1''2''4-Trichlorobenzene	120-82-1
63	六氯-1''3-丁二烯	Hexachlorobutadiene	87-68-3

Column	Rtx^®-1'' 60 m'' 0.32 mm ID'' 1.00 µm (cat.# 10157)
Sample	TO-15 standard'' injected into TO-Can^® canister and humidified to 70% RH
Conc.:	10 ppbv
Injection	sample valve
Valve Temp.:	150 °C
Oven
Oven Temp:	30 °C (hold 4 min.) to 175 °C at 9 °C/min. to 220 °C at 40 °C/min.
Carrier Gas	He'' constant flow
Flow Rate:	1.2 mL/min.
Detector	MS
Mode:	Scan
Scan Range:	35-265 amu
Preconcentrator	Nutech 3550 Preconcentrator
Trap 1 Settings
Cooling temp:	-160 °C
Desorb temp:	150 °C
Cryofocuser
Cooling temp:	-185 °C
Standard
Size:	200 mL
Instrument	HP5890 GC & 5971 MSD
Acknowledgement	Chromatogram courtesy of Gina Maio'' Severn Trent Laboratories'' Inc.'' Burlington'' VT.

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EPA TO-14/TO-15 Rtx-1