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目 录

第一章. 预启动检查 ........................................................................................... 10

1-1. 硬件 ............................................................................................................. 10

1-2. 实验调度文件（实验过程文件）.............................................................. 10

1-3. 恒电位仪模式&循环器模式 ...................................................................... 10

1-4. 虚拟控制面板 ............................................................................................. 11

1-5. 校准 ............................................................................................................. 11

第二章. 一般性说明 ........................................................................................... 12

2-1. 安装 ............................................................................................................. 12

2-1-1 硬件安装 .................................................................................................. 12

2-1-2. 软件安装 ................................................................................................. 12

2-2. 检查点 ......................................................................................................... 15

2-3. 注意事项 ..................................................................................................... 16

2-4. 前面板 ......................................................................................................... 17

2-5. 后面板 ......................................................................................................... 19

第三章. 文件菜单 ............................................................................................... 20

3-1. 打开实验条件文件 ..................................................................................... 20

3-2. 普通数据文件的ASCII文件转换 ............................................................... 24

3-3. 循环数据文件和容量数据文件的ASCII转换 ............................................ 22

3-4. 分割普通数据文件 ...................................................................................... 22

3-5. ASCII文件到二进制文件转换 .................................................................... 22

第四章. 实验菜单 ................................................................................................ 23

4-1. 电分析技术 .................................................................................................. 24

4-1-1 循环伏安法 ................................................................................................ 24

4-1-2 线性扫描伏安法 ........................................................................................ 26

4-1-3 计时安培法 ................................................................................................ 27

4-1-4 计时库仑法 ................................................................................................ 28

4-1-5 计时电位法 ................................................................................................ 29

4-1-6 方波伏安法-选配 ....................................................................................... 30

4-1-7 溶出模式–选配 ......................................................................................... 32

4-2. 直流腐蚀测量 ................................................................................................ 36

4-2-1 Tafel图 ......................................................................................................... 36

4-2-2 动态电位 ...................................................................................................... 38

4-2-3 静态电位 ...................................................................................................... 40

4-2-4 动态电流 ...................................................................................................... 42

4-2-5 静态电流 ...................................................................................................... 45

4-2-6 循环极化 ...................................................................................................... 46

4-2-7 Ecorr vs. 时间 .............................................................................................. 48

4-2-8 线性极化电阻 ............................................................................................... 49

4-2-9 Rp/Ec趋势-选配 ........................................................................................... 51

4-2-10 电偶腐蚀-选配 ............................................................................................ 53

4-3. 实验调度文件的创建 ...................................................................................... 55

4-3-1 测试信息 ........................................................................................................ 56

4-3-2 创建实验调度文件 ........................................................................................ 57

第五章 控制菜单 ..................................................................................................... 62

5-1. 监测和控制 ...................................................................................................... 62

第六章 图形菜单 ..................................................................................................... 67

6-1 基本图形功能 ................................................................................................... 68

6-1-1 用户标度 ....................................................................................................... 68

6-1-2 放大功能 ....................................................................................................... 68

6-1-3 图形网格 ....................................................................................................... 68

6-1-4 坐标值读取 .................................................................................................. 69

6-1-5 斜率计算 ..................................................................................................... 69

6-1-6 文本插入 ..................................................................................................... 70

6-1-7 ASCII转换 .................................................................................................... 70

6-1-8 复制到剪贴板 .............................................................................................. 71

6-1-9 图形格式设置 .............................................................................................. 71

6-2. 普通数据图形 ................................................................................................. 71

6-2-1 坐标轴参数 .................................................................................................. 72

6-2-2 普通数据图形的特殊绘图 .......................................................................... 74

1）仅充电图形 ....................................................................................................... 74

2）仅放电图形：同上，除了按钮不一样（红色）............................................. 75

3）充电和放电图形：+ & - 按钮按下 ................................................................... 75

4）示例 .................................................................................................................... 76

6-3 循环数据图形 .................................................................................................. 78

6-3-1 坐标轴参数 .................................................................................................. 78

6-4 阶跃数据图形 .................................................................................................. 79

第七章 报告 ............................................................................................................. 80

7-1. 循环条件文件报告 .......................................................................................... 80

7-2. 循环数据报告 ................................................................................................. 81

7-3. 容量数据报告 ................................................................................................. 82

7-4. 阶跃数据报告 ................................................................................................. 82

7-5. 校准数据报告 ................................................................................................. 83

附录 ......................................................................................................................... 84

附录1. 电解池连接 ................................................................................................ 84

A1-1 电池测试 ........................................................................................................ 84

A1-2 电化学实验和半电池测试 ............................................................................ 85

A1-3. 电偶腐蚀测试 ............................................................................................... 85

附录2. 校准 ............................................................................................................. 86

A2-1 使用外部电阻 ................................................................................................ 86

A2-2 使用简单校准套件（选配）.......................................................................... 87

A2-3 使用模拟电解池（选配）.............................................................................. 88

A2-4. 校准程序：xcalib.exe .................................................................................. 89

附录3. 工具条 .......................................................................................................... 91

附录4. 电池测试菜单-选配 ..................................................................................... 92

A4-1 里电池测试菜单 ............................................................................................. 92

A4-2 NiCd（NiMH）电池测试菜单 ...................................................................... 93

附录5. 导线和通讯模块 .......................................................................................... 94

A5-1. 电解池导线 .................................................................................................... 94

A5-3. 通讯模块 ........................................................................................................ 95